ZIMSEC O Level Combined Science Notes: Experiment: the cooling curve of naphthalene
Materials: test tube, naphthalene, thermometer, hot water, burner, stand, clamp
Be careful as naphthalene vapour is poisonous: you can wear a breathing mask to reduce the risk of you inhaling the vapour
Method
- Fill a test tube with naphthalene until it is about a quarter full
- Place the test tube in hot water to allow the naphthalene to melt
- Insert a thermometer into the test tube
- When the temperature rises above 90ºC remove the test tube from the water and clamp it
- Once the temperature begins to fall take readings every 30 seconds
- Stir the naphthalene while it is cooling
- When the temperature stops falling stop stirring as you risk breaking the thermometer
- Continue cooling until the temperature is about 30ºC
- Once the experiment is complete you will need to melt the naphthalene again so as to be able to remove the thermometer
- Plot a graph of the results
Results and observation
- The naphthalene’s temperature falls until it starts to solidify
- During the time when it is solidifying heat is given out resulting in no change in temperature
- Once the solidification process is complete the temperature of the naphthalene begins to fall again
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